The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.

该粗品通过精制工艺的改进,采用硫化钠和氢氧化钠的混合物进行处理,得到纯度≥99%的O,O-二乙基硫代磷酰氯。